[1]林碧洲.SnO2纳米晶粉的溶胶-水热合成[J].华侨大学学报(自然科学版),2000,21(3):268-270.[doi:10.3969/j.issn.1000-5013.2000.03.011]
　Lin Bizhou.Sol-Hydrothermal Synthesis of SnO2 Nano-Crystalline Powder[J].Journal of Huaqiao University(Natural Science),2000,21(3):268-270.[doi:10.3969/j.issn.1000-5013.2000.03.011]
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SnO2纳米晶粉的溶胶-水热合成()
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《华侨大学学报（自然科学版）》[ISSN:1000-5013/CN:35-1079/N]

卷:
第21卷
期数:
2000年第3期
页码:
268-270
栏目:
出版日期:
2000-07-20

文章信息/Info

Title:
Sol-Hydrothermal Synthesis of SnO2 Nano-Crystalline Powder
文章编号:
1000-5013(2000)03-0268-03
作者:
林碧洲
华侨大学化工学院, 泉州362011
Author(s):
Lin Bizhou
College of Chem. Eng., Huaqiao Univ., 362011, Quanzhou
关键词:
二氧化锡;  纳米晶粉;  溶胶-水热合成
Keywords:
tin dioxide;  nano crysta line powder;  sol hydrothermal synthesis
分类号:
TQ134.32
DOI:
10.3969/j.issn.1000-5013.2000.03.011
摘要:
以 Sn Cl4 · 5H2 O原料,用溶胶 -水热晶化复合法制备粒度较均匀,平均晶粒尺寸为 2 .5~ 4 .0nm的 Sn O2 纳米晶粉 .运用 X射线衍射 (XRD)、差热分析 (DTA)和红外吸收光谱 (IR)等分析手段对纳米晶粉进行表征 .结果表明,溶胶 -水热晶化复合法可以克服单纯水热法产率低的缺点
Abstract:
Taking SnCl 4·5H 2O as raw material,uniform sized SnO 2 nano crystalline powder with average grain size of 2.5~4.0 nm were prepared by sol hydrothermal combined method.The nano crystalline powder were characterized by applying such means as X ray diffraction, differential thermal analysis and infrared absorption spectrum.As indicated by results,the application of sol hydrothermal combined method will overcome poor yield as the weakness of single hydrothermal method.

参考文献/References:

[1] 李泉, 曾广赋, 席时权. 二氧化锡气敏材料的研究进展 [J]. 应用化学, 1994(6):1-6.
[2] Somiya S. Advanced ceramics Ⅲ [M]. London·New York, Elsevier Applied Science, 1990.207-243.
[3] 程虎民, 马季铭, 齐利民. 纳米SnO2的水热合成 [J]. 高等学校化学学报, 1995(6):833-837.
[4] Callity B D. Elements of X-ray diffraction [M]. California:Addison-Wesley Publishing Company, 1978.284-287.

更新日期/Last Update: 2014-03-23