[1]吴文士,董美斌,李宋贤.ZnCl2与POM的合成和结构[J].华侨大学学报(自然科学版),1996,17(2):136-139.[doi:10.11830/ISSN.1000-5013.1996.02.0136]
Wu Wenshi,Dong Meibing,Li Shuongxiang.Synthesis and Structure of the Addition Product of Zinc Chloride and POM[J].Journal of Huaqiao University(Natural Science),1996,17(2):136-139.[doi:10.11830/ISSN.1000-5013.1996.02.0136]
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ZnCl2与POM的合成和结构()
《华侨大学学报(自然科学版)》[ISSN:1000-5013/CN:35-1079/N]
- 卷:
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第17卷
- 期数:
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1996年第2期
- 页码:
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136-139
- 栏目:
-
- 出版日期:
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1996-04-20
文章信息/Info
- Title:
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Synthesis and Structure of the Addition Product of Zinc Chloride and POM
- 作者:
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吴文士; 董美斌; 李宋贤
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华侨大学应用化学系; 福州大学化学系
- Author(s):
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Wu Wenshi; Dong Meibing; Li Shuongxiang
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- 关键词:
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氯化锌; POM(3-甲基-4-硝基吡啶-1-氧); 加成物; 晶体结构
- Keywords:
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Zinc chloride; POM(3-methyl-4-nitropyridine-1-oxide); addition addition product; crystal structure
- 分类号:
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O641
- DOI:
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10.11830/ISSN.1000-5013.1996.02.0136
- 摘要:
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ZnCl2与POM(3-甲基-4-硝基吡啶-1-氧)生成1∶2加成物[Zn(POM)2Cl2],C12H12C12N4O6Zn,晶体属三斜晶系,空间群为P1.晶胞参数为α=11.7554(11)×10-10m,b=12.3574(7)×10-10m,c=6.5922(4)×10-10m,α=102.732(5)°,β=92.074(6)°,γ=110.124(6)°,V=876.2×10-30m,Mr=444.53,Z=2,Dx=1.70g·cm-3,μ(CuKα)=52.90cm-1,F(000)=45
- Abstract:
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An 1∶2 addition product [Zn(POM)2Cl2],C12H12Cl2N4O6 Zn is synthesized from ZnCl2 and POM (3-methyl-4-nitropyridine-1-oxide).Its crystal belongs to triclinic system,with a space group of P1. The cell parameters include:α=11.7554(11)×10-10m, b=12. 3574(7)×1
备注/Memo
- 备注/Memo:
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福建省自然科学基金
更新日期/Last Update:
2014-03-22